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The layered transition metal hydroxide based compounds M2(OH)3-x(A n- )x/nzH 2O, with M = Co, Cu, and A = organic anion, constitute a new class of organic - inorganic magnetic materials. Series of compounds are synthesized by anionic exchange reaction from transition metal hydroxide acetate or nitrate (A = OAc, NO3). This reaction induces structural change of the exchanged compounds. The combination of pow- der X-ray diffraction, infrared and UV-visible spectroscopy analyses and the analogy with known parent compounds allow to discuss the correlation between the structure and the magnetic properties. It is shown how the size and nature of the organic anion A influence strongly the properties of the bulk material. The fact that the inserted anion A coordinates the metal centers in the inorganic hydroxide based sheets induces a great interaction between the organic and inorganic subnetworks.

Structural and spectroscopic study of organic-inorganic transition metal based layered magnets