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Azadistibiranes and distibiranes formed in cycloaddition reactions of distibene [L(Me 2 N)GaSb] 2  with RN 3  and Me 3 Si(H)CN 2 . The mechanism of the reactions with PhN 3  and Me 3 SiN 3  and the electronic nature of the products were studied by DFT calculations.

Synthesis of distibiranes and azadistibiranes by cycloaddition reactions of distibenes with diazomethanes and azides