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The nickel-catalyzed olefination of benzylic dithioacetal with MeMgI or the corresponding zinc reagent generates Mg( ii ) or Zn( ii ) mercaptide which converts 2-arylpropene into dimer regioselectively.

Sequential olefination–dimerisation of benzylic dithioacetals by the nickel-catalysed reaction with methyl Grignard or zinc reagent