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A multi-component CuCo 2 S 4  and NiCo 2 S 4  thiospinel solid solution is prepared over an entire range by a low-temperature solvent-less route. The synergistic effect from both thiospinels on water splitting and capacitance is studied.

rsc advances

Tuning composition of CuCo2S4–NiCo2S4 solid solutions via solvent-less pyrolysis of molecular precursors for efficient supercapacitance and water splitting