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The first approach of photoredox catalyzed radical–radical cross-coupling difluoromethylation of C(sp 3 )−H bond was reported, featuring transition metal-free, good functional group tolerance, broad substrate scope and mild reaction conditions.

Direct C(sp3)–H difluoromethylation via radical–radical cross-coupling by visible-light photoredox catalysis

Direct C(sp³)–H difluoromethylation via radical–radical cross-coupling by visible-light photoredox catalysis