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Nd 3+  ions incorporated into hybrid layers built of [M(CN) 8 ] 4−  (M = Mo IV  or W IV ) and pyrazine  N , N ′-dioxide linkers form enantiomorphic materials exhibiting tunable NIR luminescence, SHG activity, and slow magnetic relaxation.

SHG-active NIR-emissive molecular nanomagnets generated in layered neodymium(iii)–octacyanidometallate(iv) frameworks