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Nickel phosphides were formed from Ni salt in TOPO/TOP or HDA/TOP and phase transformations from Ni 2 P to Ni 5 P 4  and  vice versa  was observed by doping with Cu or Mn salts. Doping effect on phase transition and electrocatalytic properties is studied.

Phase transformations in the nickel phosphide system induced by transition-metal doping and their electro-catalytic study