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Alkyne diimination to unsymmetric α-diimines can be achieved  via  multicomponent reaction of Ti imidos and  C -nitrosos.  C -nitroso [4 + 2] cycloaddition across a diazatitanacyclohexadiene initiates cascading retrocycloadditions, liberating the α-diimine.

α-Diimine synthesis via titanium-mediated multicomponent diimination of alkynes with C-nitrosos