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A highly enantioselective cascade  Z -selective-1,3-OH insertion/aldol cyclization of ketoacids with diazoketones involving carboxylic oxonium ylides was achieved by using a bimetallic Rh( ii )/chiral  N , N ′-dioxide-Fe( iii ) or Sc( iii ) complex catalyst.

Asymmetric synthesis of isochromanone derivatives via trapping carboxylic oxonium ylides and aldol cascade