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Using a high-temperature ball-milling technique, a practical mechanochemical protocol for the Sonogashira cross-coupling of polyaromatic halides was achieved, which provides efficient access to materials-oriented aromatic alkynes.

chemical science

Efficient access to materials-oriented aromatic alkynes <i>via</i> the mechanochemical Sonogashira coupling of solid aryl halides with large polycyclic conjugated systems

Efficient access to materials-oriented aromatic alkynes via the mechanochemical Sonogashira coupling of solid aryl halides with large polycyclic conjugated systems