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Non-polar unstrained Csp 2 –Csp 3  and Csp 2 –Csp 2  bond activation was achieved  via  B(OMe) 3 /B 2 pin 2 -mediated fragmentation borylation, in which C–C bond activation occurred regioselectively at the C2-position in various substituted indoles.

Carbon–carbon bond activation by B(OMe)3/B2pin2-mediated fragmentation borylation

Carbon–carbon bond activation by B(OMe)₃/B₂pin₂-mediated fragmentation borylation