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An intermolecular amination at the distal methylene carbon has been realized in an appended alkyl chain with electron withdrawing groups. Traceless remote C sp 3  –H functionalization has been accomplished using borate esters.

chemical science

Intermolecular CDC amination of remote and proximal unactivated C<sub>sp<sup>3</sup></sub>–H bonds through intrinsic substrate reactivity – expanding towards a traceless directing group

Intermolecular CDC amination of remote and proximal unactivated Csp3–H bonds through intrinsic substrate reactivity – expanding towards a traceless directing group

Intermolecular CDC amination of remote and proximal unactivated C_sp³–H bonds through intrinsic substrate reactivity – expanding towards a traceless directing group