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The Fe demetallation constitutes the main reason for the degradation of Fe–N–C catalysts, while previously-reported carbon surface oxidation plays a minor role. Post-annealing enables complete activity regeneration due to formation of micropores.

chemical science

Degradation and regeneration of Fe–N<sub><i>x</i></sub> active sites for the oxygen reduction reaction: the role of surface oxidation, Fe demetallation and local carbon microporosity

Degradation and regeneration of Fe–Nx active sites for the oxygen reduction reaction: the role of surface oxidation, Fe demetallation and local carbon microporosity

Degradation and regeneration of Fe–N_x active sites for the oxygen reduction reaction: the role of surface oxidation, Fe demetallation and local carbon microporosity