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A general, user-friendly approach to 2,2-disubstituted indoxyls is presented. The method is particularly useful for the preparation of 2,2-dialkylindoxyl products, and is applied to concise total syntheses of brevianamide A and trigonoliimine C.

A general approach to 2,2-disubstituted indoxyls: total synthesis of brevianamide A and trigonoliimine C