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Choice of non-coordinated diazole heteroatom in five robust triply bridged dinuclear helicates tunes  Δ  o , spin crossover and redox potential. Regardless of fraction high spin (0–0.81), DOSY NMR confirms the helicates are intact in solution.

chemical science

Correlations between ligand field Δo, spin crossover T1/2 and redox potential Epa in a family of five dinuclear helicates