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We synthesized a PbO 2 -coated electrode consisting of three layers, with Pb–0.6%Sb alloy as the substrate, α-PbO 2  as the intermediate layer, and the outermost β-PbO 2 -Co 3 O 4 @C as the active layer for boosting OER activity.

rsc advances

Two-step facile synthesis of Co3O4@C reinforced PbO2 coated electrode to promote efficient oxygen evolution reaction for zinc electrowinning