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The reaction of trimethylsilyl-substituted alkynes with 0.5 equivalents of Cp 2 ZrCl 2  and 1 equivalent of Et 3 Al in toluene at room temperature gives products of the homo-coupling in good yield.

Cp2ZrCl2 – Et3Al reagent system in the homo-coupling of trimethylsilyl-substituted alkynes

Cp₂ZrCl₂ – Et₃Al reagent system in the homo-coupling of trimethylsilyl-substituted alkynes