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For the composite catalyst, there existed synergetic catalytic effect between the hydroxyl groups and the metal center. All chain growth simultaneously proceeded between the layers or on the surface of HNTs, conducting the  in situ  ROP.

rsc advances

Microwave-assisted <i>in situ</i> ring-opening polymerization of ε-caprolactone in the presence of modified halloysite nanotubes loaded with stannous chloride

Microwave-assisted in situ ring-opening polymerization of ε-caprolactone in the presence of modified halloysite nanotubes loaded with stannous chloride