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An efficient palladium-catalyzed bisthiolation of terminal alkynes and arylhydrazines with Na 2 S 2 O 3  as the sulfur source for the assembly of ( Z )-1,2-bis(arylthio)alkene derivatives is described.

Palladium-catalyzed bisthiolation of terminal alkynes for the assembly of diverse (Z)-1,2-bis(arylthio)alkene derivatives