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Novel nickel( ii ) complexes [Ni(P,P)X2] = [Ni{  t  BuN(PPh 2 ) 2 -κ 2 P}X 2 ], X = Cl, Br, I, are prepared, characterized by IR and NMR spectroscopy, mass spectrometry and X-ray crystallography, and tested as catalysts in the Kumada cross-coupling reaction.

rsc advances

Effects of the halogenido ligands on the Kumada-coupling catalytic activity of [Ni{tBuN(PPh2)2-κ2P}X2], X = Cl, Br, I, complexes