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Three effects act as phonon scatterers: rattling of M at 8 a  cages, phase segregation, and intrinsic disorder introduced by Sn substitution, resulting in minimum  k  values. High filling fraction in Sn-doped phases pave the way to tune the carrier density in skutterudites.

rsc advances

Strongly reduced lattice thermal conductivity in Sn-doped rare-earth (M) filled skutterudites MxCo4Sb12−ySny, promoted by Sb–Sn disordering and phase segregation