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A scalable solventless approach is employed to prepare NiCo 2 S 4  and CuCo 2 S 4  with bare surface for enhanced supercapacitance and water splitting. The particles exhibit good energy storage and electrocatalytic activity as well as stability.

rsc advances

Low temperature scalable synthetic approach enabling high bifunctional electrocatalytic performance of NiCo2S4 and CuCo2S4 thiospinels