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Polymerization of VHPCS by the Grignard coupling reaction depended on the type of starting material. In the case of Cl 3 SiCH 2 Cl starting material, a stepwise growth manner was shown, due to a coupling between –CH 2 Cl and the Si–Cl sites.

Grignard coupling-based synthesis of vinyl-substituted hydridopolycarbosilane: effect of starting material and polymerization behavior