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Complexation of tripodal ligands with silver(I) salts generated M 3 L 2  cage complexes that encapsulated anions within their cavities. Subsequent [N–Ag–N] +  to [N–I–N] +  cation exchange with I 2  resulted in the corresponding halogen-bonded iodine(I) cages.

inorganic chemistry frontiers

Dimeric iodine(<scp>i</scp>) and silver(<scp>i</scp>) cages from tripodal N-donor ligands via the [N–Ag–N]+ to [N–I–N]+ cation exchange reaction

Dimeric iodine(i) and silver(i) cages from tripodal N-donor ligands via the [N–Ag–N]+ to [N–I–N]+ cation exchange reaction

Dimeric iodine(i) and silver(i) cages from tripodal N-donor ligands via the [N–Ag–N]⁺ to [N–I–N]⁺ cation exchange reaction