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Synchrotron radiation X-ray micro-analytical techniques and vibrational micro-spectroscopy methods were used to establish the factors and mechanism of darkening of “fake-gilded” decorations in the  Maestà  by Cimabue and aged paint mock-ups.

journal of analytical atomic spectrometry

Development of a multi-method analytical approach based on the combination of synchrotron radiation X-ray micro-analytical techniques and vibrational micro-spectroscopy methods to unveil the causes and mechanism of darkening of “fake-gilded” decorations in a Cimabue painting