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A series of symmetrical and unsymmetrical rhodium( iii ) bis-boryl complexes [(PMe 3 ) 3 Rh(boryl) 2 Cl] and [(PMe 3 ) 3 Rh(boryl) 2 L][BArF] (L = PMe 3 , MeCN, MeNC; boryl = Bcat, Bpin) are synthesised and spectroscopically and structurally characterised.

Ligand properties of boryl ligands in bis-boryl rhodium(iii) complexes: a case study