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Intercalation of lithium and ammonia into the layered semiconductor Bi 2 Se 3  proceeds  via  a hyperextended (by >60%) ammonia-rich intercalate, to eventually produce a layered compound with lithium amide intercalated between the bismuth selenide layers which offers scope for further chemical manipulation.

Intercalates of Bi2Se3 studied in situ by time-resolved powder X-ray diffraction and neutron diffraction

Intercalates of Bi₂Se₃ studied in situ by time-resolved powder X-ray diffraction and neutron diffraction