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Crystal structures of new rubidium rare earth thiophosphates with the formulas Rb 3 Ln(PS 4 ) 2  (Ln = La, Ce, Pr), Rb 3−x Na x Ln(PS 4 ) 2  (Ln = Ce, Pr;  x  = 0.50, 0.55), and RbEuPS 4  crystallized out of a molten RbCl flux.

crystengcomm

Trends in rare earth thiophosphate syntheses: Rb3Ln(PS4)2 (Ln = La, Ce, Pr), Rb3−xNaxLn(PS4)2 (Ln = Ce, Pr; x = 0.50, 0.55), and RbEuPS4 obtained by molten flux crystal growth