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A Pd-catalyzed C(sp 3 )–C(sp) bond formation for the direct functionalization of cyclobutenes with alkynes has been achieved, suggesting (DFT and control experiments) an unusual pathway of oxidative addition in tertiary iodoalkanes.

Pd-catalyzed C(sp3)–C(sp) bond formation in iodocyclobutenes

Pd-catalyzed C(sp³)–C(sp) bond formation in iodocyclobutenes