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Drawing on independent work carried out by academic and industrial researchers using the immobilized TEMPO catalyst Silia Cat  TEMPO, in this study, we show how shifting the carboxylation process mediated by TEMPO in solution to a process mediated by the above-mentioned hybrid sol–gel catalyst allows the synthesis of insoluble polysaccharide nanofibers of superior quality, eliminating waste.

Enhanced polysaccharide nanofibers via oxidation over SiliaCat TEMPO