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Here we provide definitive EPR evidence for the existence of α-triphenylstannylvinyl radicals such as  (Z)-2  in the low temperature O-directed free radical hydrostannation of dialkyl propargylic alcohols with Ph 3 SnH/cat. Et 3 B and O 2  in PhMe.

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EPR evidence for α-triphenylstannylvinyl radicals in the O-directed hydrostannation of dialkylacetylenes with Ph3SnH/cat. Et3B/O2