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The targeted synthesis of the α- and β-like polymorph of Na 4 P 2 S 6 , characterization of subtle structural changes, and the impact on sodium-ion diffusion is demonstrated.

Phase formation through synthetic control: polymorphism in the sodium-ion solid electrolyte Na4P2S6

Phase formation through synthetic control: polymorphism in the sodium-ion solid electrolyte Na₄P₂S₆