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An unprecedented tandem [4 + 2]/[2 + 2] cycloaddition of  o -carboryne with enynes has been disclosed for the efficient synthesis of various carborane-fused tricyclics, in which a reactive carborane-fused 1,2-cyclohexadiene intermediate is involved.

Tandem [4 + 2]/[2 + 2] cycloaddition of o-carboryne with enynes: facile construction of carborane-fused tricyclics