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A mechanistically distinct Ni-catalysed benzylic functionalization of indoles is developed by the facile oxidation of arenes. The method exhibits a wide substrate scope and pronounced chemoselectivity that cannot be accessed  via  known protocols.

Benzylic C(sp3)–C(sp2) cross-coupling of indoles enabled by oxidative radical generation and nickel catalysis

Benzylic C(sp³)–C(sp²) cross-coupling of indoles enabled by oxidative radical generation and nickel catalysis