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The merger of manganese-catalyzed C–H functionalization with electrosynthesis enabled C(sp 3 )–H azidation devoid of chemical oxidants or photochemical irradiation. Detailed mechanistic studies are supportive of a manganese( iii/iv ) electrocatalysis.

Mangana(iii/iv)electro-catalyzed C(sp3)–H azidation

Mangana(iii/iv)electro-catalyzed C(sp³)–H azidation