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A reversible carbon–boron bond formation has been observed in the reaction of the coordinatively unsaturated, cyclometalated, Pt( ii ) complex [Pt(I  t  Bu i Pr′)(I  t  Bu i Pr)][BAr F ], 1, with tricoordinated boranes HBR 2 .

Reversible carbon–boron bond formation at platinum centers through σ-BH complexes