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We describe an example of a two-electron metal- and ligand-based reduction of Me 3 SiN 3  using uranium( iv ) complexes with varying steric properties. With uranium-based reduction, a U( vi ) intermediate is isolated.

Divergent uranium- versus phosphorus-based reduction of Me3SiN3 with steric modification of phosphido ligands

Divergent uranium- versus phosphorus-based reduction of Me₃SiN₃ with steric modification of phosphido ligands