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We present the facile synthesis of Ni/NiO nanocomposites,  via  a solution combustion methodology, where the composition of metallic Ni within NiO is controlled by varying the annealing time, from 4 minutes up to 8 hours.

Facile synthesis of Ni/NiO nanocomposites: the effect of Ni content in NiO upon the oxygen evolution reaction within alkaline media