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A series of 2-ethoxycarbonylthieno[2,3- b ]quinolines were synthesized in the bio-derived “green” solvent γ-valerolactone and evaluated for their inhibitory activities against PTP1B, compound 6a displayed an IC 50 value of 8.04 ± 0.71 μM with 4.34-fold preference over TCPTP.

rsc advances

Synthesis of 2-ethoxycarbonylthieno[2,3-<i>b</i>]quinolines in biomass-derived solvent γ-valerolactone and their biological evaluation against protein tyrosine phosphatase 1B

Synthesis of 2-ethoxycarbonylthieno[2,3-b]quinolines in biomass-derived solvent γ-valerolactone and their biological evaluation against protein tyrosine phosphatase 1B