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In this work, an outstanding nanolayered tin phosphate with 15.0 Å interlayer spacing, Sn (HPO 4 ) 2 ·3H 2 O (SnP–H + ), has been synthesized by conventional hydrothermal method and first used in the adsorptive removal of Cr( iii ) from aqueous solution.

Hydrothermal synthesis of a novel nanolayered tin phosphate for removing Cr(iii)