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PdCl 2  (3 mol%)/XantPhos (6 mol%) complexes was found to be a highly efficient catalyst for the synthesis of 2-alkenylbenzo[ b ]furans from 2 - bromobenzo[ b ]furans and alkenylaluminums. The reaction was also found to be effective in gram-scale synthesis.

Palladium-catalyzed cross-coupling reaction of alkenyl aluminums with 2-bromobenzo[b]furans