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Nanoscale resolution X-ray spectromicroscopy shows the co-incubation of β-amyloid (Aβ) and iron( iii ) to result in aggregate structures displaying nanoscale heterogeneity in Aβ and iron chemistry, including the formation of potentially cytotoxic Fe 0 .

Nanoscale chemical speciation of β-amyloid/iron aggregates using soft X-ray spectromicroscopy