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Stoichiometrically and sequentially optimized periodate–chlorite oxidations generate tunable C2,C3 dialdehyde–dicarboxylate CNFs/CNCs for tough amphiphilic and wet shape recoverable aerogels.

nanoscale advances

Tunable dialdehyde/dicarboxylate nanocelluloses by stoichiometrically optimized sequential periodate–chlorite oxidation for tough and wet shape recoverable aerogels