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The clathrate-I borosilicide K 8−x B y Si 46−y  (0.8 ≤  x  ≤ 1.2 and 6.4 ≤  y  ≤ 7.2; space group  Pm 3̄ n ) was prepared in sealed tantalum ampoules between 900 °C and 1000 °C.

The impact of boron atoms on clathrate-I silicides: composition range of the borosilicide K8−xBySi46−y

The impact of boron atoms on clathrate-I silicides: composition range of the borosilicide K_8−xB_ySi_46−y