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A large  S -shaped [MnIII5MnII2] 2  assembly (∼40 Å top to tail) has been formed with bis- p - t Bu-calix[4]arene and 2-(hydroxymethyl)pyridine as a co-ligand, with the former existing unusually in both  syn  and  anti -conformations (as shown).

With complements of the ligands: an unusual S-shaped [Mn7]2 assembly from tethered calixarenes

With complements of the ligands: an unusual S-shaped [Mn₇]₂ assembly from tethered calixarenes