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A Transition Anionic Complex (TAC) was formed and passed into [P 6,6,6,14 ][BOB] when Li[BOB] (but not Na[BOB]) was used in the synthesis, significantly altering ILs' properties. The TAC transformed into [BOB] −  in the IL upon heating at 413 K for 1 h.

Transition anionic complex in trihexyl(tetradecyl)phosphonium-bis(oxalato)borate ionic liquid – revisited