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We present synchrotron-based mass spectrometry to probe products formed in a lithium sulphide electrolyte. In operando analysis was carried out at two different potentials in a vacuum compatible microfluidic electrochemical cell. Mass spectral observations show that the charged electrolyte formed sulphur clusters under dynamic conditions, demonstrating electrolyte electron shuttling.

Probing sulphur clusters in a microfluidic electrochemical cell with synchrotron-based photoionization mass spectrometry