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The cross-coupling of aryl bromides with [ 11 C]CH 3 Li for the labelling of a variety of tracers for positron emission tomography (PET) is presented. The radiolabelled products were obtained in excellent yields, at rt and after short reaction times (3-5 min) compatible with the half-life of 11 C (20.4 min). The automation of the protocol on a synthesis module is investigated, representing an important step towards a fast method for the synthesis of 11 C-labelled compounds for PET imaging.

Cross-coupling of [11C]methyllithium for 11C-labelled PET tracer synthesis

Cross-coupling of [¹¹C]methyllithium for ¹¹C-labelled PET tracer synthesis