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Addition of HOTf to a mixture of Co III (BDPP)(O 2 ˙) ( 1 ) and Cp* 2 Fe produced H 2 O 2  in high yield implying formation of Co III (BDPP)(OOH) ( 3 ), and reaction of Sc(OTf) 3  with the same mixture gave a peroxo-bridged Co III /Sc III  5 .

Ambiphilicity of a mononuclear cobalt(iii) superoxo complex