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Here, we report the quantitative electroreduction of CO2 to CO by a PNP-pincer iridium(i) complex bearing amino linkers in DMF/water. The electrocatalytic properties greatly depend on the choice of linker within the ligand. The complex 3-N is far superior to the analogues with methylene and oxygen linkers, showing higher activity and better selectivity for CO2 over proton reduction.

Surprisingly big linker-dependence of activity and selectivity in CO2 reduction by an iridium(i) pincer complex

Surprisingly big linker-dependence of activity and selectivity in CO₂ reduction by an iridium(i) pincer complex